HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Oxopropyl)benzoyl chloride → 1-(4-Carboisopropoxyphenyl)propan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Oxopropyl)benzoyl chloride | HCID 20134178 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 1-(4-Carboisopropoxyphenyl)propan-2-one | HCID 20134177 | — |
Reaction Steps
Isopropanol (30 ml) was added to 4-acetonylbenzoyl chloride (2.61 g) and the solution left at room temperature 3 days. Removal of the solvent gave the title compound as an oil. γ (CDCl3) 8.66 (3H, d, J=7 Hz), 7.88 (3H, s), 6.28 (2H, s), 4.78 (1H, h, J=7 Hz), 2.80 (2H, d, J=9 Hz) 2.04 (2H, d, J=9 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04753962 |
| Source dataset | uspto-grants-1988_06 |
| ORD ID | ord-2b618e91ac3c4b489d43117c85efbcca |
| Source note | uspto-grants-1988_06 |