Water → HCID 13326123, compound

Participants

Reaction Steps

An equimolar amount of potassium tert.-butylate is added to 54.6 g (0.1 mole) of the tosylate of 1,1-bis-(2,4-dichlorophenoxy)-3,3-dimethylbutan-2-ol in 200 ml of dry dimethylsulfoxide. The mixture is stirred for 30 minutes at room temperature, after which it is hydrolyzed with water and then extracted twice with the same volume of ethyl acetate, the organic phase is dried and the solvent is distilled off under reduced pressure.

Provenance & Evidence