Butyl nitrite → HCID 53842386, compound

Participants

Reaction Steps

To a solution of 4, 5-di-(2-chloropyridin-3-yl)-2-aminooxazole (0.030 g) in tetrahydrofuran (3 mL) was added butylnitrite (0.033 g). The mixture was heated under reflux for 3 hours. The solvent was evaporated, and the residue was fractionated by chromatography to give 4, 5-di-(2-chloropyridin-3-yl)oxazole (0.010 g) as a solid. mp 157-158° C.

Provenance & Evidence