Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 67594327 | HCID 67594327 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54556780 | HCID 54556780 | — |
Reaction Steps
A solution of the alcohol 67 (1 mmole) in THF is cooled to 0° C. Methanesulfonyl chloride (1 mmole) and triethylamine (1 mmole) are added and the solution is stirred at 0° C. for 6 hr. Standard work-up and flash chromatography affords 68.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05919797 |
|---|
| Source dataset | uspto-grants-1999_07 |
|---|
| ORD ID | ord-3f2baf8cbad5402984dc274555748e9d |
|---|
| Source note | uspto-grants-1999_07 |
|---|
