HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 67623488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Nicotinic acid, hydrazide | HCID 11112 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 15858800 | HCID 15858800 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67623488 | HCID 67623488 | — |
Reaction Steps
Next, 0.33 g of 5,6,7,8-tetrahydro-2-(3-nitrophenyl)-3-formylimidazo[2,1-b]benzothiazol, 0.15 g of nicotinohydrazide, and 0.1 g of potassium hydroxide were heated and stirred in 20 ml of methanol at 90° C. for 1.5 hours. After cooling, water was added and the desired substance was obtained in an amount of 0.21 g (yield of 46.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05919799 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-a906c8b2c5a94183801339f6b90ba210 |
| Source note | uspto-grants-1999_07 |