Acetic Acid → HCID 54561915, compound

Participants

Reaction Conditions

Reaction Steps

0.45 g (2 mmol) of 2-benzylmercapto-6-hydroxy-benzothiazole are dissolved in 15 ml of warm glacial acetic acid and at 50° C. 2.5 ml of 35% hydrogen peroxide is added. The mixture is stirred for 1 hour at 50° C. and 20 minutes at 100° C. It is then added to water, neutralised with soda and extracted with ethyl acetate. The extracts are dried and evaporated down. The evaporation residue is digested with a little ether and suction filtered. Yield: 60.6% of theory, Melting point: 188-189° C.

Provenance & Evidence