Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trimethylsilyl isocyanate → ((4-Aminophenyl)methyl)urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trimethylsilyl isocyanate | HCID 70696 | — |
| 반응물 | 4-Aminobenzylamine | HCID 427814 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | ((4-Aminophenyl)methyl)urea | HCID 40423978 | — |
반응 단계
Trimethylsilylisocyanate (3.2 ml; 85%) was added to a solution of 4-amino-benzylamine (1.55 ml) in dry THF (40 ml). A white solid precipitated. The reaction mixture was stirred at r.t. overnight then the precipitate was filtered and washed with ethyl acetate giving the title compound (1.2 g) as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05919811 |
| 출처 데이터셋 | uspto-grants-1999_07 |
| ORD ID | ord-e22ede468ecd4eb0b42b6c8623ae3b4c |
| 출처 메모 | uspto-grants-1999_07 |