HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 53739331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18404153 | HCID 18404153 | — |
| Reactant | HCID 178527775 | HCID 178527775 | — |
| Product | HCID 53739331 | HCID 53739331 | — |
Reaction Steps
According to the procedure indicated in Example A1, reaction of 2-mercapto-1H-benzimidazole with 4-(2-chloroethylthio)-2-chloromethyl-3-methylpyridine hydrochloride and NaOH gives, after crystallization from ethyl acetate, the title compound (62% of theory) as a colorless solid of m.p. 178-180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922720 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-b2a13a6151d142fea86b7228220bea59 |
| Source note | uspto-grants-1999_07 |