HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 10991979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 11032782 | HCID 11032782 | — |
| Reactant | HCID 178516507 | HCID 178516507 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 10991979 | HCID 10991979 | — |
Reaction Steps
0.4 g 2-(5-Chloro-2-thienyl)-4,6-dichloropyrimidine, 0.2 g 2-Chloro-4-hydroxypyridine, and 0.3 g potassium carbonate are refluxed in 30 mL dry acetonitrile for 16 hours. The mixture is poured into water, and the product is extracted with toluene and purified by flash chromatography (0.38 g, m.p. 154-156° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922726 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-22478c799aa44c9886ca41bdf4ea6e13 |
| Source note | uspto-grants-1999_07 |