HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 178452058, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 178472379 | HCID 178472379 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 178452058 | HCID 178452058 | — |
Reaction Steps
Prepared from ethyl trans-4-[[-4-[1-(tert-butyloxycarbonyl)-piperidin-4-yl]-piperazin-1-yl]-carbonyl]-cyclohexane-carboxylate by hydrolysis with lithium hydroxide analogously to Example 24. Mass spectrum: (M+H)+ =424; Rf value: 0.24 (silica gel; methylene chloride/methanol/concentrated ammonia=4:1:0.2)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922717 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-83c6fe1cd0fa4c558b65b7eb032a8bdc |
| Source note | uspto-grants-1999_07 |