HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178501118, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 178511262 | HCID 178511262 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178501118 | HCID 178501118 | — |
Reaction Steps
A solution of 15.7 g of trans-4-(aminomethyl)-cyclohexanecarboxylic acid in 150 ml of ethereal hydrochloric acid and 1000 ml of absolute methanol is stirred at room temperature for 20 hours. The solvent is evaporated off under reduced pressure and the residue is triturated with ether and filtered off with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922717 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-cd63c4a4dcdf409f87b1e3f94366e5d1 |
| Source note | uspto-grants-1999_07 |