HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(2-Bromoethyl)cyclopent-1-ene → 1-(2-Cyclopent-2-en-1-ylethyl)-6-(3,5-dimethylbenzoyl)-5-isopropyl-pyrimidine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(2-Bromoethyl)cyclopent-1-ene | HCID 12658866 | — |
| Reactant | 6-(3,5-Dimethyl-benzoyl)-5-isopropyl-1H-pyrimidine-2,4-dione | HCID 22256582 | — |
| Product | 1-(2-Cyclopent-2-en-1-ylethyl)-6-(3,5-dimethylbenzoyl)-5-isopropyl-pyrimidine-2,4-dione | HCID 483494 | 32.3% |
Reaction Steps
5-Isopropyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione and 2-(cyclopent-2-en-1-yl)ethyl bromide were reacted by the same method with example 40 to obtain the titled compound (123 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922727 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-ee92c283b7e1430cb09fe4025f7ca6a6 |
| Source note | uspto-grants-1999_07 |