HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 581901Generated: October 30, 2026
Benzeneseleninic acid → HCID 53770367, compound
https://huagongshe.com/reaction/581901
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzeneseleninic acid | HCID 23427 | — |
| Reactant | HCID 54564593 | HCID 54564593 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 53770367 | HCID 53770367 | — |
Reaction Steps
A mixture of 27 from Example 6 (3.9 g, 12.9 mmol) and benzeneseleninic acid (3.04 g, 16.1 mmol) in toluene is stirred at 70° C. over night. The product precipitates upon cooling. The precipitate is filtered off, washed with petroleum ether and dried. Subsequent washings with aqueous sodium carbonate and water affords pure 28. Yield: 2.99 g (77%). Mp 179-181° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05922725 |
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| Source dataset | uspto-grants-1999_07 |
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| ORD ID | ord-3f6038fdb8b548b8b0cf2ebda0bc4af3 |
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| Source note | uspto-grants-1999_07 |
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