HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Methylhydroxylamine hydrochloride → HCID 87417072, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| Reactant | 5-Formyl-1-(3-(4-pyrimidyl)phenyl)benzimidazole | HCID 53950824 | — |
| Product | HCID 87417072 | HCID 87417072 | 28.1% |
Reaction Steps
was synthesized as described in Example 22 but using (62) (200 mg, 0.66 mmol) instead of (55) and NH2OMe.HCl (250 mg, 2.0 mmol). The reaction gave (64) (61 mg, 28%). Mp. 180-182° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922725 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-3e944dcefd484bb68d56dd7699de8040 |
| Source note | uspto-grants-1999_07 |