HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → 1-(4-amino-3-nitrophenyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | n-(4-Acetyl-2-nitrophenyl)acetamide | HCID 286549 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-(4-amino-3-nitrophenyl)ethanone | HCID 11586389 | — |
Reaction Steps
N-(4-acetyl-2-nitrophenyl)acetamide (26.5 g, 11.94 mmol) was added to a mixture of water and concentrated sulfuric acid, 150 ml (1:2). After 15 minutes the mixture was poured into water. The product was filtered off, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922724 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-4cd9d2f8740145f98a89fec295a82ac8 |
| Source note | uspto-grants-1999_07 |