HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70347532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-(4-(Methylsulfonyl)phenyl)-2-(3-pyridinyl)-2-cyclopenten-1-one | HCID 9796843 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70347532 | HCID 70347532 | — |
Reaction Steps
To a solution of 3-(4-(methylsulfonyl)phenyl)-2-(3-pyridinyl)-2-cyclopenten-1-one (5.0 g, 15.96 mmol) in CH2Cl2 (50 mL) was passed a stream of HCl gas for 10 min. Excess HCl was removed by bubbling a stream of air through the solution. The solution was then concentrated and swished in Et2O to give 5.7 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922742 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-d177aa9e1096408ea3a6d985ea612dd1 |
| Source note | uspto-grants-1999_07 |