HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → HCID 70189071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | HCID 70189085 | HCID 70189085 | — |
| Product | HCID 70189071 | HCID 70189071 | 81% |
Reaction Steps
(E)-2-(5-Bromo-6-methoxyindan-1-ylidene)ethylamine (5.0 g, 18.6 mmol) was dissolved in saturated HCl/ethanol (200 ml) and the solution was refluxed for 2 hours. After cooling, the solvent was distilled off under reduced pressure and the resulting crystals were washed with diethyl ether to provide the title compound (yield 4.61 g, 81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05922771 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-fb9c0479f8634848ab81cac23ff26593 |
| Source note | uspto-grants-1999_07 |