Oxalyl chloride → HCID 19598110, compound

HRID 582365Notes

Reaction equation

HRID 582365 reaction equation
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([O:12][CH3:13])=[C:6]([C:10]=1[Cl:11])[C:7](O)=[O:8].C(Cl)(=O)C([Cl:17])=O>ClCCl>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([O:12][CH3:13])=[C:6]([C:10]=1[Cl:11])[C:7]([Cl:17])=[O:8]

Participants

4

Reactant 2

HCID 65578Oxalyl chlorideHCID 19598108HCID 19598108, compound

Product 1

HCID 19598110HCID 19598110, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A mixture of 4B (1.2 g, 4.6 mmol), dichloromethane (15 ml) and oxalyl chloride (1 ml) is stirred at room temperature for 2 hours. The mixture is concentrated and the resulting benzoylchloride is used without further purification.

Workup

  1. concentrationThe mixture is concentrated
  2. customthe resulting benzoylchloride is used without further purification

Sources & evidence

ORD record
ord-2058ba2cce5c4ce8945a57efdbcddf46
Source dataset
uspto-grants-1999_07
Patent number
US05922905

Reaction notes

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