反应详情

温度

-10 °C

N-phenyl furamide was prepared by adding to a mixture of aniline (23.3 g; 250 mmol) and triethylamine (25.3 g; 250 mmol) in dichloromethane slowly 32.6 g (250 mmol) of 2-furoyl chloride, while maintaining the temperature at -10° C. The product obtained was washed with diluted hydrochloric acid and water, dried with magnesium sulphate and evaporated. The product so obtained was than triturated with hexane and filtered. 39.3 g (84% yield of product was recovered.

1. customThe product obtained
2. washwas washed with diluted hydrochloric acid and water
3. dry with materialdried with magnesium sulphate
4. customevaporated
5. customThe product so obtained
6. customthan triturated with hexane
7. filtrationfiltered