HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19602468, compound → HCID 19602501, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19602468 | HCID 19602468 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 19602501 | HCID 19602501 | — |
Reaction Steps
(3RS, 5SR)-3-azidomethyl-4-oxa-1-azabicyclo [3,2,0] heptan-7-one (150 mg, 0.89 mmol) was hydrogenated with 100 mg of 10% palladium on activated carbon in 25 ml of ethyl acetate at 50 psi hydrogen pressure at room temperature for 1 hr. After removal of catalyst by filtration, (3RS, 5SR)-3-aminomethyl-4-oxa-1-azabicyclo [3,2,0] heptan-7-one in ethyl acetate was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05925633 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-d20e13dcc89d4ee0aaa59e43cfb9eafd |
| Source note | uspto-grants-1999_07 |