Sodium Hydroxide → HCID 86754261, compound

Participants

Reaction Steps

A methanol solution (25 mL) of 5-2 (328 mg, 0.61 mmol) and 1N NaOH (5 mL, 5 mmol) was stirred under ambient conditions overnight. The reaction was concentrated to dryness and the residue dissolved in H2O and the solution acidified with 6 N HCl to provide 5-3 as a solid.

Provenance & Evidence