Sodium Hydroxide → HCID 86754268, compound

Participants

Reaction Steps

A methanol solution (3 mL) of 8-2 (184 mg, 0.34 mmol) and 1 N NaOH (3.4 mL, 3.4 mmol) was stirred under ambient conditions for 3 h. The reaction was concentrated to dryness and the residue dissolved in H2O and neutralized with 1 N HCl to provide 8-3 as a solid.

Provenance & Evidence