Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 582791Generated: October 30, 2026

Phosphoric Acid → HCID 70246175, compound

https://huagongshe.com/reaction/582791

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhosphoric AcidHCID 1004—
ReactantSR142948AHCID 5311451—
SolventEthanolHCID 702—
SolventDichloromethaneHCID 6344—
ProductHCID 70246175HCID 7024617535%

Reaction Conditions

Temperature50 °C

Reaction Steps

A mixture of 0.1 g of the compound obtained in EXAMPLE 1' and 0.017 g of 85% orthophosphoric acid in 2 ml of DCM and 3 ml of EtOH is left stirring for 1 hour at. RT. It is partially concentrated under vacuum and poured into 10 ml of ether cooled to 50° C., and the precipitate formed is drained. 0.04 g of the expected product is obtained after drying at 60° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05925661
Source datasetuspto-grants-1999_07
ORD IDord-feb957ddf2a34cb88d6f54fd3d636d67
Source noteuspto-grants-1999_07