HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Diethoxy-1-propanol → 3,3-Diethoxy-1-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Diethoxy-1-propanol | HCID 140135 | — |
| Reactant | Naphthalene potassium | HCID 66602812 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3,3-Diethoxy-1-propanol | HCID 140135 | — |
| Product | Potassium | HCID 5462222 | — |
Reaction Steps
A reactor was charged with 30 ml of THF, 0.13 g of 3, 3-diethoxypropanol and 2 ml solution of potassium naphthalene dissolved in tetrahydrofuran in a concentration of 0.5 mol/L-tetrahydrofuran, and the resulting mixture was stirred for three minutes in an argon atmosphere, and, thus, there was formed a potassium derivative (potassium 3, 3-diethoxypropanoxide) of 3, 3-diethoxypropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05925720 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-04bb0291bcd64345a483338c57e0abaa |
| Source note | uspto-grants-1999_07 |