Hydrogen Bromide → 4-(1-Bromoethyl)-1,2-dichlorobenzene

HRID 582923Notes

Reaction equation

HRID 582923 reaction equation
[BrH:1].[Cl:2][C:3]1[CH:4]=[C:5]([CH:10](O)[CH3:11])[CH:6]=[CH:7][C:8]=1[Cl:9]>CC(O)=O>[Br:1][CH:10]([C:5]1[CH:6]=[CH:7][C:8]([Cl:9])=[C:3]([Cl:2])[CH:4]=1)[CH3:11]

Participants

4

Reactant 2

HCID 260Hydrogen BromideHCID 978993,4-Dichloro-alpha-methylbenzenemethanol

Product 1

HCID 431414504-(1-Bromoethyl)-1,2-dichlorobenzene

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

This compound is prepared by the procedure described in Preparation 3.4 from 25 ml of a 33% solution of HBr in AcOH and 5 g of 3,4-dichloro-1-(1-hydroxyethyl)benzene. 6.4 g of the expected product are obtained.

Workup

  1. customThis compound is prepared by the procedure

Sources & evidence

ORD record
ord-a19af4c3ad4349fbbd94bf22f1d2e7db
Source dataset
uspto-grants-1999_07
Patent number
US05925768

Reaction notes

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