Butyl isocyanate → HCID 54048187, compound

HRID 582944Notes

Reaction equation

HRID 582944 reaction equation
[OH:1][N:2]1[C:7]([CH3:9])([CH3:8])[CH2:6][CH:5]([NH2:10])[CH2:4][C:3]1([CH3:12])[CH3:11].[CH2:13]([N:17]=[C:18]=[O:19])[CH2:14][CH2:15][CH3:16]>C1(C)C=CC=CC=1>[CH2:13]([NH:17][C:18]([NH:10][CH:5]1[CH2:6][C:7]([CH3:8])([CH3:9])[N:2]([OH:1])[C:3]([CH3:12])([CH3:11])[CH2:4]1)=[O:19])[CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 8110Butyl isocyanateHCID 8459714691-88-4

Product 1

HCID 54048187HCID 54048187, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

To a stirred solution of 1.0 g of 1-oxyl-4-amino-2,2,6,6-tetramethylpiperidine in 75 mL of dry toluene is added dropwise 0.65 mL of butyl isocyanate. The reaction mixture is stirred for 16 hours. The solution is then concentrated to yield the title compound as a red oil.

Workup

  1. concentrationThe solution is then concentrated

Sources & evidence

ORD record
ord-39c3d63dc36b41bda9d049fa45e330f1
Source dataset
uspto-grants-1999_07
Patent number
US05928558

Reaction notes

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