HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl isocyanate → HCID 54048187, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl isocyanate | HCID 8110 | — |
| Reactant | Tempamine H | HCID 84597 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54048187 | HCID 54048187 | — |
Reaction Steps
To a stirred solution of 1.0 g of 1-oxyl-4-amino-2,2,6,6-tetramethylpiperidine in 75 mL of dry toluene is added dropwise 0.65 mL of butyl isocyanate. The reaction mixture is stirred for 16 hours. The solution is then concentrated to yield the title compound as a red oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05928558 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-39c3d63dc36b41bda9d049fa45e330f1 |
| Source note | uspto-grants-1999_07 |