HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → (3-nitro-2-oxopyridin-1(2H)-yl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | tert-Butyl 3-nitro-2-oxo-1(2H)-pyridineacetate | HCID 18989321 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | (3-nitro-2-oxopyridin-1(2H)-yl)acetic acid | HCID 607739 | — |
Reaction Steps
3.73 g (14.7 mmol) of tert-butyl 2-(3-nitro-2-oxopyridin-1(2H)-yl)acetate are dissolved in 10 mL of dichloromethane and treated with 40 mL of trifluoroacetic acid. It is stirred at
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09434763B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-04a2184d04ee4e7faef12ebbbf8e2be1 |
| Source note | uspto-grants-2016_09 |