HCID 70126930, compound → HCID 70128349, compound

Participants

Reaction Steps

7-Nitro-1-methyl-3,4-dihydro-1H-benzo[e][1,4]diazapine hydrochloride (3.2 g, 13.1 mmol) was dissolved in methanol (100 ml) and hydrogenated at 50 psi in the presence of a catalytic quantity of 10% Pd--C. After 1 h the mixture was filtered through glass and evaporated to an oil which was used immediately in the next reaction.

Provenance & Evidence