Trifluoroacetic acid → HCID 178484701, compound

Participants

Reaction Steps

N2—{(E)-[(tert-butoxycarbonyl)amino][(tert-butoxycarbonyl)imino]methyl}-N2-methyl-N-[3-(triphenylphosphonio)propyl]glycinamide bromide (290 mg, 0.41 mmol) was dissolved in trifluoroacetic acid (1 ml, 10 mmol). After 20 minutes at room temperature, the volatiles were removed under vacuum, and the crude was purified with reverse phase preparative HPLC to give the title compound in a 31% yield.

Provenance & Evidence