HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70055432, compound → HCID 21310911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70055432 | HCID 70055432 | — |
| Solvent | Methylenechloride Hexane | HCID 21226440 | — |
| Product | HCID 21310911 | HCID 21310911 | 90.3% |
Reaction Steps
In the same manner as described in Example 19, 1.86 g (3.6 mmol) of the product of Example 97 provided 1.39 g (90%) of the desired carboxylic acid as a white solid after trituration with CH2Cl2 :hexane (1:4). CI Mass Spec 428.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929097 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-6731f8045e084cdeb51a71993589f12f |
| Source note | uspto-grants-1999_07 |