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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 583319Generated: October 31, 2026

Methanol → HCID 21310919, compound

https://huagongshe.com/reaction/583319

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 70053518HCID 70053518—
SolventDiethyl EtherHCID 3283—
ProductHCID 21310919HCID 2131091993%

Reaction Steps

In the same manner as described in Example 19, except a mixture of MeOH and ThF was used instead of MeOH, 0.506 g (1.1 mmol) of the product of Example 98 provided 0.454 g (93%) of the desired carboxylic acid as a white solid after triion with ether. Electrospray Mass Spec 446.1(M+H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05929097
Source datasetuspto-grants-1999_07
ORD IDord-be4d8c9546b743cf8265ba87b30725d5
Source noteuspto-grants-1999_07