HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 21310919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 70053518 | HCID 70053518 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21310919 | HCID 21310919 | 93% |
Reaction Steps
In the same manner as described in Example 19, except a mixture of MeOH and ThF was used instead of MeOH, 0.506 g (1.1 mmol) of the product of Example 98 provided 0.454 g (93%) of the desired carboxylic acid as a white solid after triion with ether. Electrospray Mass Spec 446.1(M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929097 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-be4d8c9546b743cf8265ba87b30725d5 |
| Source note | uspto-grants-1999_07 |