HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzyl bromide → HCID 15859218, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Reactant | HCID 53963569 | HCID 53963569 | — |
| Solvent | Diethylether hexane | HCID 21584099 | — |
| Product | HCID 15859218 | HCID 15859218 | 86.4% |
Reaction Steps
In the same manner as described in Example 9, 0.699 g (2.0 mmol) of the product of Example 62 and 0.6 g (2.4 mmol) of p-bromobenzyl bromide provided 0.896 g (86%) of the desired product as a white solid after trituration with hexane/ether. Electrospray Mass Spec 518.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929097 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-9d91dd06907e45da96d67b8a25b37f92 |
| Source note | uspto-grants-1999_07 |