Iodoethane → HCID 70053935, compound

HRID 583334Notes

Reaction equation

[CH3:1][O:2][C:3](=[O:24])[C:4]1[CH:9]=[C:8]([CH3:10])[CH:7]=[C:6]([CH3:11])[C:5]=1[NH:12][S:13]([C:16]1[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][CH:17]=1)(=[O:15])=[O:14].I[CH2:26][CH3:27]>>[CH3:1][O:2][C:3](=[O:24])[C:4]1[CH:9]=[C:8]([CH3:10])[CH:7]=[C:6]([CH3:11])[C:5]=1[N:12]([CH2:26][CH3:27])[S:13]([C:16]1[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][CH:17]=1)(=[O:15])=[O:14]

Participants

Reactant 2

HCID 6340Iodoethane

HCID 53963569HCID 53963569, compound

Product 1

HCID 70053935HCID 70053935, compoundYield 100%

Procedure

In the same manner as described in Example 9, 0.30 g (0.860 mmol) of the product of Example 62 and 0.103 mL (1.289 mmol) of iodoethane provided 0.324 g (100%) of the desired product as a white solid. Electrospray Mass Spec 378.2(M+H).

Sources & evidence

ORD record: ord-e01d0f3be9c34b7c9165be46cfa4c3d2
Source dataset: uspto-grants-1999_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05929097

Reaction notes

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