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HRID58353

反应详情

EQUATION

反应方程式

HRID 58353 的结构方程式

REACTANTS

反应物

2
结构：[I-].[Na+]
HCID5238

Sodium Iodide

INa

结构：CCO[Si](CCCSCCCCCCOC(=O)C(C)(C)Br)(OCC)OCC
HCID123835937

未命名化合物

PRODUCTS

生成物

1
结构：CCO[Si](CCCSCCCCCCOC(=O)C(C)(C)I)(OCC)OCC
HCID123825932

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

The 6-(3-(triethoxysilyl)propylthio)hexyl 2-bromo-2-methylpropanate (5 g) obtained through the procedures of Example 1 was mixed with sodium iodide (20 g) and dry acetone (100 mL), and the mixture was allowed to react in a nitrogen atmosphere at 75° C. for 10 hours. After the reaction, extraction was performed to give 6-(3-(triethoxysilyl)propylthio)hexyl 2-iodo-2-methylpropanate of the chemical formula below (compound 6).

WORKUP

后处理

  1. customto react in a nitrogen atmosphere at 75° C. for 10 hours
  2. customAfter the reaction, extraction