HCID 21311168, compound → HCID 54092533, compound

Participants

Reaction Steps

A solution of 5.1 grams of 5-vinyl-5-nonanol in 25 ml of toluene containing 38 mg of MTO was refluxed overnight, cooled, washed with aq. potassium carbonate, dried, stripped, and the residue distilled at 25 mm Hg to give 2.55 g (56%) of 5-vinyl-4-nonene as a cis/trans mixture, identified by NMR spectroscopy.

Provenance & Evidence