HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → HCID 18928616, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | HCID 18928608 | HCID 18928608 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18928616 | HCID 18928616 | — |
Reaction Steps
Thiourea (374 mg, 4.9 mmol) and 21-2 (1.4 g, 4.7 mmol) were combined in 24 mL EtOH and heated to reflux for 1 h. Concentration and flash chromatography (silica, 80% EtOAc/hexane then 10% MeOH/EtOAc) provided 21-3 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929120 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-ae9e6e75c93d4b45913593f12efee7b2 |
| Source note | uspto-grants-1999_07 |