HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 10255701, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 10603017 | HCID 10603017 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10255701 | HCID 10255701 | — |
Reaction Steps
A solution of 32-6 (221 mg, 0.39 mmol), TFA (5 mL) and CH2Cl2 (50 mL) was stirred under ambient conditions for 18 h. The reaction was concentrated and the solid residue purified by flash chromatography (silica, 19:1 EtOH/NH4OH) to give 32-7 as a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929120 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-1f232eb1e7b8402b892956ec474103c3 |
| Source note | uspto-grants-1999_07 |