HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfur → HCID 70109822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfur | HCID 5362487 | — |
| Reactant | HCID 54346156 | HCID 54346156 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70109822 | HCID 70109822 | — |
Reaction Steps
A mixture of 36-4 (2.5 g, 7.0 mmol), HgO (3.0 g, 13.9 mmol), sulfur (42 mg) and EtOH (50 mL) was refluxed for 2.5 h. Filtration and concentration gave a brown gum which was purified by flash chromatography (silica, 9:1 CH2Cl2 /CH3OH) to provide 36-5 as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05929120 |
| Source dataset | uspto-grants-1999_07 |
| ORD ID | ord-668f76c9095b4c29bff14c25cef7872f |
| Source note | uspto-grants-1999_07 |