Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 22342518 | HCID 22342518 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 69693809 | HCID 69693809 | — |
Reaction Steps
A mixture of 3-methoxy-thiophene-2,5-dicarboxylic acid (0.382 g), benzylamine (0.41 mL), N,N′-carboxyl≈diimidazole (0.66 g), and DMF was heated at 60° C. to yield 0.39 g of 3-methoxy-thiophene-2,5-dicarboxylic acid bis benzylamide; MI-APCI+ 381.1; Elem. Anal. (C21H20N2O3S); Calc'd: C, 66.30; H, 5.30; N, 7.36. Found: C, 66.52; H, 5.06; N, 7.41.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06924276B2 |
|---|
| Source dataset | uspto-grants-2005_08 |
|---|
| ORD ID | ord-2524547aeeba4a1cb901c8497647047d |
|---|
| Source note | uspto-grants-2005_08 |
|---|
