HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopropane → 4-(4-Chloro-3-trifluoromethyl-phenyl)-1-propyl-piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | 4-[4-Chloro-3-(trifluoromethyl)phenyl]piperidine | HCID 16679317 | — |
| Product | 4-(4-Chloro-3-trifluoromethyl-phenyl)-1-propyl-piperidine | HCID 9904611 | — |
Reaction Steps
Beginning with 4-(4-Chloro-3-trifluoromethyl-phenyl)-piperidine and 1-propyliodide, the title compound was re-covered by the procedure described in Example 2. m.p. 218-220° C. (HCl), MS m/z (rel. intensity, 70 eV) 305 (M+, 4), 278 (35), 277 (13), 276 (bp), 70 (40).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924374B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-1d117724a1404b918824579f3281b741 |
| Source note | uspto-grants-2005_08 |