HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → cis-4-(3,4-Dichloro-phenyl)-2,6-dimethyl-1-propyl-piperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-Bromo-1,2-dichlorobenzene | HCID 29013 | — |
| Reactant | (2R,6S)-2,6-Dimethyl-1-propylpiperazine | HCID 28363798 | — |
| Product | cis-4-(3,4-Dichloro-phenyl)-2,6-dimethyl-1-propyl-piperazine | HCID 68444886 | — |
Reaction Steps
Beginning with 4-bromo-1,2-dichlorobenzene and cis-2,6-dimethyl-1-propyl-piperazine, the title compound was recovered by the procedure described in Preparation 9: m.p. 225° C. (HCl), MS m/z (rel. intensity, 70 eV)) 301 (M+, 24), 271 (64), 112 (bp), 70 (47), 56 (53).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924374B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-762c182daf1343518215c56ff0ec539c |
| Source note | uspto-grants-2005_08 |