Hydrochloric Acid → HCID 22345178, compound

HRID 584079Notes

Reaction equation

HRID 584079 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH2:9][CH2:10][N:11]([CH2:14][CH2:15][CH3:16])[CH2:12][CH:13]=2)=[CH:4][C:3]=1[C:17]([F:20])([F:19])[F:18].Cl>>[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH2:13][CH2:12][N:11]([CH2:14][CH2:15][CH3:16])[CH2:10][CH2:9]2)=[CH:4][C:3]=1[C:17]([F:20])([F:18])[F:19]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 22345153HCID 22345153, compound

Product 1

HCID 22345178HCID 22345178, compound

Procedure

Beginning with 4-(4-Fluoro-3-trifluoromethylphenyl)-1-propyl-1,2,3,6-tetrahydropyridine, the titled compound was recovered by the procedure described in Preparation 6: m.p. 195-197° C. (HCl), MS m/z (rel. intensity, 70 eV)) 289 (M+, 4), 261 (15), 260 (bp), 177 (7), 70 (13).

Workup

  1. customthe titled compound was recovered by the procedure
  2. customdescribed in Preparation 6

Sources & evidence

ORD record
ord-dae596b4015e4055b9a2b4939380fa8d
Source dataset
uspto-grants-2005_08
Patent number
US06924374B2

Reaction notes

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