1-Iodopropane → HCID 22345187, compound

HRID 584081Notes

Reaction equation

HRID 584081 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[S:14]([CH3:17])(=[O:16])=[O:15].I[CH2:19][CH2:20][CH3:21]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:9][CH2:10][N:11]([CH2:19][CH2:20][CH3:21])[CH2:12][CH2:13]2)=[CH:4][C:3]=1[S:14]([CH3:17])(=[O:15])=[O:16]

Participants

3

Reactant 2

HCID 336431-IodopropaneHCID 22345190HCID 22345190, compound

Product 1

HCID 22345187HCID 22345187, compound

Procedure

Beginning with 1-(4-Chloro-3-methanesulfonyl-phenyl)-piperazine and 1-iodopropane, the titled compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV)) 316 (M+, 25), 289 (41), 287 (bp), 70 (59), 56 (23)

Workup

  1. customthe titled compound was recovered by the procedure

Sources & evidence

ORD record
ord-4a4ab50323404816867bd71f93d27a7d
Source dataset
uspto-grants-2005_08
Patent number
US06924374B2

Reaction notes

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