HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 22343040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 22343414 | HCID 22343414 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22343040 | HCID 22343040 | 58% |
Reaction Steps
To 2,2-dimethyl-2,3-dihydro-1H-4,9a-diaza-fluoren-9-one (1.5 g, 7.0 mmol) in EtOH (17.5 mL), hydrazine hydrate (0.98 mL) was added and the mixture was heated at reflux for 3½ h. Crystallization provided 0.994 g (58%) of 4-(3-amino-2,2-dimethyl-propylamino)-2H-phthalazin-1-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924284B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-e2428fae6eaf45a1a96fe7631cb4dd1d |
| Source note | uspto-grants-2005_08 |