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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 584120Generated: November 2, 2026

Succinic anhydride → HCID 22343117, compound

https://huagongshe.com/reaction/584120

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSuccinic anhydrideHCID 7922—
ReactantHCID 178513305HCID 178513305—
SolventDimethylformamideHCID 6228—
ProductHCID 22343117HCID 2234311771%

Reaction Conditions

Temperature120 °C

Reaction Steps

Succinic anhydride (0.39 g, 3.89 mmol) and 6-chloro-N-hydroxy-nicotinamidine (0.67 g, 3.89 mmol) were dissolved in 2 mL of DMF and heated at 120° C. for 2 h. The cooled solution was filtered and the precipitate was washed with water, and dried to give the product as 0.70 g (71%) of colorless solid which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06924284B2
Source datasetuspto-grants-2005_08
ORD IDord-290283f69cef4c44ad0dd7811f34642d
Source noteuspto-grants-2005_08