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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 584131Generated: November 1, 2026

Diisopropylethylamine → HCID 22343051, compound

https://huagongshe.com/reaction/584131

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropylethylamineHCID 81531—
ReactantHCID 22343088HCID 22343088—
ReactantHCID 22343439HCID 22343439—
SolventDimethylformamideHCID 6228—
ProductHCID 22343051HCID 22343051—

Reaction Steps

To a solution of 4-chloromethyl-2H-phthalazin-1-one (9.7 mg, 0.05 mmol) in DMF (200 μL), N-(2-amino-ethyl)-3-[3-(4-methoxy-phenyl)-[1,2,4]oxadiazol-5-yl]-propionamide (14.4 mg, 0.05 mmol) and DIPEA (9 μL, 0.05 mmol) were added. The mixture was stirred overnight at rt and directly applied to preparative HPLC. The purity was determined by RPLC/MS.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06924284B2
Source datasetuspto-grants-2005_08
ORD IDord-9a25e25318c94fdea5cdd8d2e2184e8b
Source noteuspto-grants-2005_08