HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 22343051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 22343088 | HCID 22343088 | — |
| Reactant | HCID 22343439 | HCID 22343439 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22343051 | HCID 22343051 | — |
Reaction Steps
To a solution of 4-chloromethyl-2H-phthalazin-1-one (9.7 mg, 0.05 mmol) in DMF (200 μL), N-(2-amino-ethyl)-3-[3-(4-methoxy-phenyl)-[1,2,4]oxadiazol-5-yl]-propionamide (14.4 mg, 0.05 mmol) and DIPEA (9 μL, 0.05 mmol) were added. The mixture was stirred overnight at rt and directly applied to preparative HPLC. The purity was determined by RPLC/MS.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924284B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-9a25e25318c94fdea5cdd8d2e2184e8b |
| Source note | uspto-grants-2005_08 |