HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10012515, compound → HCID 22342827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10012515 | HCID 10012515 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22342827 | HCID 22342827 | 104% |
Reaction Steps
A solution of ethyl (E)-3-(1-methyl-1H-imidazol-4-yl)acrylate (2.5 g) in tetrahydrofuran (100 ml) was hydrogenated over 10% palladium activated carbon (0.2 g) at room temperature under 2 atmospheric pressure. After removal of catalyst by filtration through Celite pad, the filtrate was concentrated under reduced pressure to give ethyl 3-(1-methyl-1H-imidazol-4-yl)propionate (2.63 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924278B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-54437d5a158441fa907f050c1ce2a195 |
| Source note | uspto-grants-2005_08 |