HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-N,N-2-trimethylpropenylamine → HCID 22345557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-N,N-2-trimethylpropenylamine | HCID 640792 | — |
| Reactant | 4-(((1,1-Dimethylethoxy)carbonyl)amino)-1-methyl-1H-imidazole-2-carboxylic acid | HCID 2757226 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 22345557 | HCID 22345557 | — |
Reaction Steps
N-(1-chloro-2-methylprop-1-enyl)-N,N-dimethylamine (660 μL, 4.99 mmol) was added to a mixture of 1-methyl-4-(BOC amino)imidazole-2-carboxylic acid (1.00 g, 4.17 mmol) in CHCl3 (8.00 mL). After a few minutes, the 1H-NMR of the reaction mixture showed complete conversion of the acid to the acid chloride. 1H NMR (CDCl3): δ 7.48 (br s, 1H), 3.95 (s, 3H), 1.50 (s, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924396B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-2642c50ef1d44d9c9b2c4cd89d27a905 |
| Source note | uspto-grants-2005_08 |