HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Bromophenyl)acrylic acid → HCID 69792460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Bromophenyl)acrylic acid | HCID 36251 | — |
| Reactant | HCID 22345372 | HCID 22345372 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | HCID 69792460 | HCID 69792460 | 62% |
Reaction Steps
In a manner similar to that of Example 1(c), by reaction of 3.4 g (11.6 mmol) of 1-methoxymethoxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthaleneboronic acid with 1.32 g (5.8 mmol) of 3-bromocinnamic acid, trituration in heptane gave 1.4 g (62%) of 3-[3-(1-methoxymethoxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthyl)phenyl]acrylic acid in the form of a white powder having a melting point of 188°-9° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06924388B2 |
| Source dataset | uspto-grants-2005_08 |
| ORD ID | ord-a096bad5b5c54fc08ef8a216caa326bc |
| Source note | uspto-grants-2005_08 |